Complexometric determination of thallium(III) using ethanethiol as a selective masking agent

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Complexometric Determination of Thallium(III) using Ethanethiol as a Selective Masking Agent

Um método complexométrico simples e seletivo é proposto para a determinação de tálio na presença de outros metais, pela habilidade do etanetiol em mascarar seletivamente íons tálio (III). Em solução, o tálio presente foi inicialmente complexado com um excesso conhecido de EDTA, sendo o excesso titulado com uma solução padrão de sulfato de zinco em pH 5-6 (hexamina), usando-se xilenol como indic...

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Indirect Complexometric Determination of Mercury Using Potassium Iodide as Selective Masking Agent

This paper describes a indirect complexometric method for the determination of mercury in the presence of co-ions, based on the selective masking ability of potassium iodide. To the mixture of mercury (II) and other metal ion solution, EDTA solution was added in excess of the metal ions present. The pH of the solution was adjusted to 5.0-6.0 using solid hexamine (10 ± 2 g) and surplus EDTA was ...

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Selective masking and demasking for the stepwise complexometric determination of aluminium, lead and zinc from the same solution

BACKGROUND A complexometric method based on selective masking and de-masking has been developed for the rapid determination of aluminium, lead and zinc from the same solution in glass and glass frit samples. The determination is carried out using potassium cyanide to mask zinc, and excess disodium salt of EDTA to mask lead and aluminium. The excess EDTA was titrated with standard Mn(II)SO(4 )so...

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Improved Extraction-Separation of Lanthanum/ Europium Ions by Bis(2-ethylhexyl)phosphoric Acid Using 12-Crown-4 as an Ion Selective Masking Agent

The extraction-separation of lanthanum and europium ions with bis(2-ethylhexyl) phosphoric acid (DEHPA) in cyclohexane was improved by adding 12-crown-4 (12C4) to the aqueous phase as a masking agent. In the presence of this crown ether the extraction curve of lanthanum ions versus pH shifts to the higher pH region, while the curve is not influenced for the europium ions. Consequently the s...

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Complexometric Determination of Hydroxyzinium Chloride

The conditions of preparation of hydroxyziniurn tetraiodocadmiatewere elaborated. The chemical composition and solubility were determined as well as thermal analysis was performed. Basi ng on the spectrophotometric investigations the mechanism of hydroxyziniumtetraiodocadmiate formation was established. The method of the complexometric determination of hydroxyzinium chloride, within the concent...

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ژورنال

عنوان ژورنال: Journal of the Brazilian Chemical Society

سال: 2006

ISSN: 0103-5053

DOI: 10.1590/s0103-50532006000200014